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- W2015951971 abstract "Reaktion der Cardenolidsteroide 1,2,5 und 6 mit 2,3,4-Tri-O-benzoyl-α-L-rhamnopyranosylbromid oder mit 2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosylbromid in Gegenwart von Quecksilber(II)-cyanid führt zur Glykosidierung der tertiären 3-Hydroxygruppe. Anschließende Abspaltung der Schutzgruppen ergibt an C-3 verzweigte, herzwirksame Glykoside in 50 bis 60 proz. Gesamtausbeute. Synthesis of Glycosides of C-3 Branched Cardenolides Reaction of cardenolide steroids 1,2,5, and 6 with 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide or 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide in the presence of mercury(II) cyanide leads to glycosidation of the tertiary 3-hydroxy group. Subsequent hydrolysis of protecting groups gives C-3 branched, cardioactive glycosides in 50—60% overall yield." @default.
- W2015951971 created "2016-06-24" @default.
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- W2015951971 date "1977-11-11" @default.
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- W2015951971 title "Synthese von Glykosiden C-3-verzweigter Cardenolide" @default.
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- W2015951971 doi "https://doi.org/10.1002/jlac.197719770904" @default.
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