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• W2016020513 abstract "The reproducibility and bias of the measurement of column efficiency from chromatographic peaks were studied. Peaks of various signal-to-noise and τ/σ ratios, a measure of the asymmetry of a peak, were generated by computer simulation. A range of experimental peaks were also analyzed. Column efficiencies for a variety of peaks were computer calculated, using eight commonly employed methods. The results are compared. The moment method gave the best results in almost all instances of noisy or skewed peaks, except in the simulated noisy cases with a signal-to-noise ratio of less than 40, and seems to be the most accurate method for the measurement of column efficiency for those with access to a computer for calculations. The most common method, the half-height method, surprisingly seems fairly sensitive to noise fluctuations, and di not perform as well as some of the other methods, including the 3σ, 4σ and 5σ methods, in the most noisy instances." @default.
• W2016020513 created "2016-06-24" @default.
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• W2016020513 date "1988-01-01" @default.
• W2016020513 modified "2023-09-26" @default.
• W2016020513 title "Effect of random noise and peak asymmetry on the precision and accuracy of measurements of the column efficiency in chromatography" @default.
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• W2016020513 doi "https://doi.org/10.1016/s0021-9673(01)82051-3" @default.
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