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- W2016031386 abstract "Abstract Eine Reihe von Lanthanoid(III)‐amiden [Ln{N(C 6 H 5 )(SiMe 3 )} 3 (THF) x ] [Ln = Y ( 1 ), La ( 2 ), Nd ( 3 ), Sm ( 4 ), Eu ( 5 ), Tb ( 6 ), Er ( 8 ), Yb ( 9 ), Lu ( 10 )] wurde durch Reaktion der entsprechenden Lanthanoidtrichloride, LnCl 3 , mit LiN(C 6 H 5 )(SiMe 3 ) erhalten. Die Umsetzung von NdCl 3 (THF) 2 und LuCl 3 (THF) 3 mit den Lithiumsalzen der sterisch anspruchsvollen Amide [N(C 6 H 3 R 2 ‐2,6)(SiMe 3 )] − (R = Me, iso ‐Pr) führt zur Bildung der Lanthanoiddiamide [Li(THF) 2 (μ‐Cl) 2 Nd{N(C 6 H 3 Me 2 ‐2, 6)(SiMe 3 )} 2 (THF)] ( 11 ) und [ClLn{N(C 6 H 3 ‐ iso ‐Pr 2 ‐2,6)(SiMe 3 )} 2 (THF)] [Ln = Nd ( 12 ), Lu ( 13 )]. Die neuen Verbindungen wurden durch 1 H‐ und 13 C‐NMR‐ und Massenspektren, die Neodymderivate 3, 11 und 12 durch Röntgenstrukturanalysen charakterisiert." @default.
- W2016031386 created "2016-06-24" @default.
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- W2016031386 date "1995-01-01" @default.
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- W2016031386 title "Metallorganische Verbindungen der Lanthanoide. 88. Monomere Lanthanoid(III)-amide: Synthese und R�ntgenstrukturanalyse von [Nd{N(C6H5)(SiMe3)}3(THF)], [Li(THF)2(?-Cl)2Nd{N(C6H3Me2-2,6)(SiMe3)}2(THF)] und [ClNd{N(C6H3-iso-Pr2-2,6)(SiMe3)}2(THF)]" @default.
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- W2016031386 doi "https://doi.org/10.1002/zaac.19956210123" @default.
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