Matches in SemOpenAlex for { <https://semopenalex.org/work/W2016036384> ?p ?o ?g. }
Showing items 1 to 98 of
98
with 100 items per page.
- W2016036384 endingPage "135" @default.
- W2016036384 startingPage "130" @default.
- W2016036384 abstract "In the current paper, we report the development of a new capillary electrophoresis method using pre-column derivatization and laser-induced fluorescence detection for the determination of ephedrine and amphetamine drugs. Our new method allows for the identification and quantification of six commonly used illicit drugs namely pseudoephedrine, ephedrine, amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, and 3,4-methylenedioxymethylamphetamine, respectively, as well as propafenone (internal standard). Following derivatization with fluorescein isothiocyanate, a total of six amphetamine drugs and the internal standard could readily be separated using a fused-silica 75 micromID x 60 cm length (effective length: 50.2 cm) capillary column. The mobile phase consisted of buffer containing 20mM borate (pH 12, adjusted with sodium hydroxide). Samples were injected in pressure mode with the capillary being operated at 25kV/25 degrees C, and the detection of the derivatized compounds was sought using a laser-induced fluorescence (LIF) detector (lambda(ex)=488 nm and lambda(em)=520 nm), with a run-time of 20 min. The current method was validated with regard to precision (relative standard deviation, RSD), accuracy, sensitivity, linear range, limit of detection (LOD) and limit of quantification (LOQ). In human blood and urine samples, detection limits were 0.2 ngmL(-1), and the linear range of the calibration curves was 0.5-100 ngmL(-1). The intra-day and inter-day precisions were both less than 13.22%." @default.
- W2016036384 created "2016-06-24" @default.
- W2016036384 creator A5014602567 @default.
- W2016036384 creator A5024735954 @default.
- W2016036384 creator A5025598270 @default.
- W2016036384 creator A5066716873 @default.
- W2016036384 date "2007-09-15" @default.
- W2016036384 modified "2023-09-24" @default.
- W2016036384 title "Capillary electrophoresis with laser-induced fluorescence and pre-column derivatization for the analysis of illicit drugs" @default.
- W2016036384 cites W1973819421 @default.
- W2016036384 cites W1984480138 @default.
- W2016036384 cites W1991128243 @default.
- W2016036384 cites W2014190716 @default.
- W2016036384 cites W2031760529 @default.
- W2016036384 cites W2039852686 @default.
- W2016036384 cites W2047445302 @default.
- W2016036384 cites W2068079310 @default.
- W2016036384 cites W2082395255 @default.
- W2016036384 cites W2084695872 @default.
- W2016036384 cites W2088979850 @default.
- W2016036384 cites W2098721205 @default.
- W2016036384 cites W2144822880 @default.
- W2016036384 cites W2982925530 @default.
- W2016036384 doi "https://doi.org/10.1016/j.jchromb.2007.07.009" @default.
- W2016036384 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17689300" @default.
- W2016036384 hasPublicationYear "2007" @default.
- W2016036384 type Work @default.
- W2016036384 sameAs 2016036384 @default.
- W2016036384 citedByCount "25" @default.
- W2016036384 countsByYear W20160363842012 @default.
- W2016036384 countsByYear W20160363842013 @default.
- W2016036384 countsByYear W20160363842014 @default.
- W2016036384 countsByYear W20160363842015 @default.
- W2016036384 countsByYear W20160363842016 @default.
- W2016036384 countsByYear W20160363842017 @default.
- W2016036384 countsByYear W20160363842018 @default.
- W2016036384 countsByYear W20160363842021 @default.
- W2016036384 crossrefType "journal-article" @default.
- W2016036384 hasAuthorship W2016036384A5014602567 @default.
- W2016036384 hasAuthorship W2016036384A5024735954 @default.
- W2016036384 hasAuthorship W2016036384A5025598270 @default.
- W2016036384 hasAuthorship W2016036384A5066716873 @default.
- W2016036384 hasConcept C10349863 @default.
- W2016036384 hasConcept C10390740 @default.
- W2016036384 hasConcept C113196181 @default.
- W2016036384 hasConcept C119128265 @default.
- W2016036384 hasConcept C121332964 @default.
- W2016036384 hasConcept C1342733 @default.
- W2016036384 hasConcept C162356407 @default.
- W2016036384 hasConcept C169760540 @default.
- W2016036384 hasConcept C185592680 @default.
- W2016036384 hasConcept C23531484 @default.
- W2016036384 hasConcept C2776923573 @default.
- W2016036384 hasConcept C2778984665 @default.
- W2016036384 hasConcept C2900643 @default.
- W2016036384 hasConcept C43617362 @default.
- W2016036384 hasConcept C62520636 @default.
- W2016036384 hasConcept C86803240 @default.
- W2016036384 hasConcept C91881484 @default.
- W2016036384 hasConceptScore W2016036384C10349863 @default.
- W2016036384 hasConceptScore W2016036384C10390740 @default.
- W2016036384 hasConceptScore W2016036384C113196181 @default.
- W2016036384 hasConceptScore W2016036384C119128265 @default.
- W2016036384 hasConceptScore W2016036384C121332964 @default.
- W2016036384 hasConceptScore W2016036384C1342733 @default.
- W2016036384 hasConceptScore W2016036384C162356407 @default.
- W2016036384 hasConceptScore W2016036384C169760540 @default.
- W2016036384 hasConceptScore W2016036384C185592680 @default.
- W2016036384 hasConceptScore W2016036384C23531484 @default.
- W2016036384 hasConceptScore W2016036384C2776923573 @default.
- W2016036384 hasConceptScore W2016036384C2778984665 @default.
- W2016036384 hasConceptScore W2016036384C2900643 @default.
- W2016036384 hasConceptScore W2016036384C43617362 @default.
- W2016036384 hasConceptScore W2016036384C62520636 @default.
- W2016036384 hasConceptScore W2016036384C86803240 @default.
- W2016036384 hasConceptScore W2016036384C91881484 @default.
- W2016036384 hasIssue "1" @default.
- W2016036384 hasLocation W20160363841 @default.
- W2016036384 hasLocation W20160363842 @default.
- W2016036384 hasOpenAccess W2016036384 @default.
- W2016036384 hasPrimaryLocation W20160363841 @default.
- W2016036384 hasRelatedWork W2001142110 @default.
- W2016036384 hasRelatedWork W2016036384 @default.
- W2016036384 hasRelatedWork W2017308769 @default.
- W2016036384 hasRelatedWork W2071002483 @default.
- W2016036384 hasRelatedWork W2099217060 @default.
- W2016036384 hasRelatedWork W2380019247 @default.
- W2016036384 hasRelatedWork W2389167103 @default.
- W2016036384 hasRelatedWork W242352810 @default.
- W2016036384 hasRelatedWork W2808213894 @default.
- W2016036384 hasRelatedWork W4205172216 @default.
- W2016036384 hasVolume "857" @default.
- W2016036384 isParatext "false" @default.
- W2016036384 isRetracted "false" @default.
- W2016036384 magId "2016036384" @default.
- W2016036384 workType "article" @default.