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• W2016058546 abstract "6Li MAS NMR has been used to study the lithium local environments and manganese electronic structures of a number of lithium manganese oxides with manganese oxidation states varying from (III) to (IV). Most samples were chosen with compositions within the LiMn2O4−Li2Mn4O9−Li4Mn5O12 phase diagram, but Li2Mn2O4 with Mn(III) was also synthesized for comparison. Despite the presence of unpaired electrons, high-resolution spectra could still be acquired, allowing a number of different local environments to be detected. Assignments of the resonances to different lithium local environments were made by comparing the observed shifts and local structures in a number of lithium manganates. Two 6Li NMR resonances were observed for the spinel phase Li4Mn5O12 at 1980 and 847 ppm, which were assigned to Li+ in the octahedral and tetrahedral sites of the spinel structure, respectively. A shift was observed for Li+ in the tetrahedral site of Li2Mn4O9, which also contains Mn(IV), at 687 ppm. The shifts are ascribed primar..." @default.
• W2016058546 created "2016-06-24" @default.
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• W2016058546 creator A5079933241 @default.
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• W2016058546 date "1998-11-19" @default.
• W2016058546 modified "2023-09-27" @default.
• W2016058546 title "⁶Li and ⁷Li MAS NMR Studies of Lithium Manganate Cathode Materials" @default.
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• W2016058546 doi "https://doi.org/10.1021/ja9817794" @default.
• W2016058546 hasPublicationYear "1998" @default.
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