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• W2016068583 abstract "A comparison of the reactivity of (acylamino)-nitroso-pyrimidines 1 and the alkenylamino analogue 17 in intramolecular ene reactions showed the considerably lower reactivity of 17, leading to the pteridine 18. Pteridin-7-one 11 resulting from 1 (R-1 = OBn, R-2 = Me) was transformed into 4-(benzyloxy)-6-[(E)-prop-1-enyl] pteridin-2-amine (13) by O-triflation, followed by reduction with LiBHEt3, while the 4-MeO analogue 18 was prepared by spontaneous oxidation of the initial ene product of 17. The (alkenylamino)-nitroso-pyrimidine 17 was synthesized by substitution of the dimethoxy-nitroso-pyrimidine 16 with the allylamine 15. Ciliapterin (5) and dictyopterin (7) were synthesized from pteridine 18 by a Sharpless asymmetric dihydroxylation." @default.
• W2016068583 created "2016-06-24" @default.
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• W2016068583 date "2008-12-01" @default.
• W2016068583 modified "2023-09-26" @default.
• W2016068583 title "A New Synthesis of Ciliapterin and Dictyopterin. Ene Reactions of (Alkenylamino)-nitroso-pyrimidines" @default.
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• W2016068583 doi "https://doi.org/10.1002/hlca.200890255" @default.
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