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• W2016069673 abstract "Phase relations, composition dependence of lattice constants, structure refinement, and electrical resistivity of the mixed-metal compounds, (V,Mo)3S4, are presented. Phase relationships in the system VMoS were studied by sealed silica tube experiments at 1373 K and an isothermal section of the phase diagram was constructed. The system VMoS is characterized by the following three solid solution series: cubic metal alloy VxMo1−x (0 ≤ x ≤ 1), monoclinic (VxMo1−x)2.06S3 (0 ≤ x ≤ 0.06), and monoclinic V3−xMoxS4 (0 ≤ x ≤ 2). The (V,Mo)3S4 phase coexists with MoS2 at higher S content, while it coexists with Mo at lower S content. The structures of VMo2S4 and V2MoS4 were determined and refined from X-ray powder data. A monoclinic Cr3S4-type cell with space group I2m was adopted. It was found that the contraction of the lattice constant b on substitution of Mo for V in (V,Mo)3S4 mixed crystals is due to formation of characteristic zigzag MoMo chains running along the b direction of the lattice. With respect to the metal distribution of Mo and V in the Cr3S4-type structure, Mo atoms have a great tendency to occupy metal sites in the metal-filled layers rather than those in the metal-deficient layers." @default.
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• W2016069673 date "1986-07-01" @default.
• W2016069673 modified "2023-10-18" @default.
• W2016069673 title "Phase relations and structure of V3−xMoxS4 (0 ≤ x ≤ 2)" @default.
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• W2016069673 doi "https://doi.org/10.1016/0022-4596(86)90193-3" @default.
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