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• W2016095965 abstract "Abstract A novel open‐tubular capillary electrochromatography (OTCEC) column was prepared by immobilizing dodecanethiol gold nanoparticles on prederivatised fused‐silica capillary columns with sol‐gel technology. 3‐Mercaptopropyl‐trimethoxysilane (MPTMS) was selected as sol‐gel precursor to develop a sol‐gel layer on the inner wall of the capillary, prior to assembly of dodecanethiol gold nanoparticles onto the generated sol‐gel layer through specific interaction between the gold nanoparticles and surface terminating thiol groups. The electrochromatographic behaviour of the sol‐gel gold nanoparticle capillary was compared with a gold nanoparticle capillary prepared via MPTMS surface functionalisation, through variation of the percentage of the organic modifier, pH, and separation voltage. Efficient separation for a “reversed‐phase” test mixture of thiourea, naphthalene, and biphenyl and for selected polycyclic aromatic hydrocarbons (PAHs) was obtained on the sol‐gel based gold nanoparticle capillaries. OTCEC separations of three selected drug substances (propiophenone, benzoin, and warfarin) were also demonstrated. Scanning electron microscopy was used for the characterization of the sol‐gel gold nanoparticle capillary surface. The results confirm that dodecanethiol gold nanoparticles, bound on the sol‐gel‐based inner layer of fused‐silica capillary, can provide sufficient solute‐bonded phase interactions for OTCEC with reproducible retention as well as characteristic reversed‐phase behaviour." @default.
• W2016095965 created "2016-06-24" @default.
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• W2016095965 date "2005-05-01" @default.
• W2016095965 modified "2023-09-27" @default.
• W2016095965 title "Alkylthiol gold nanoparticles in sol-gel-based open tubular capillary electrochromatography" @default.
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• W2016095965 doi "https://doi.org/10.1002/jssc.200400075" @default.
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