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- W2016099864 abstract "1,1-Diamino-2,2-dinitroethene, C2H4N4O4 (FOX-7), is a novel high energy density material with low friction and impact sensitivity and a high activation barrier to detonation. In this study, the previously unknown crystal structure of the γ-polymorph of trimorphic FOX-7 is reported. γ-FOX-7 is stable from ∼435 K until the compound decomposes just above 504 K. A single crystal of α-FOX-7 (P21/n, Z=4, a=694.67(7) pm, b=668.87(9) pm, c=1135.1(1) pm, β=90.14(1)°, T=373 K) was first transformed into a single crystal of β-FOX-7 (P212121, Z=4, a=698.6(1) pm, b=668.6(2) pm, c=1168.7(3) pm, T=423 K) and then into a single crystal of γ-FOX-7 at 450 K. The γ-FOX-7 crystal was then subsequently quenched to 200 K. The structure of γ-FOX-7 (P21/n, Z=8, a=1335.4(3) pm, b=689.5(1) pm, c=1205.0(2) pm, β=111.102(8)°, T=200 K) consists of four planar layers, each containing two crystallographically independent FOX-7 molecules found in the asymmetric unit." @default.
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- W2016099864 date "2007-12-01" @default.
- W2016099864 modified "2023-10-02" @default.
- W2016099864 title "γ-FOX-7: Structure of a High Energy Density Material Immediately Prior to Decomposition" @default.
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- W2016099864 doi "https://doi.org/10.1002/prep.200700240" @default.
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