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- W2016104013 abstract "Abstract Brown single crystals of PbMnF 5 were obtained by tempering a mixture of PbF 2 and MnF 3 in sealed gold tubes at 550°C for ten days. Crystal data: M r = 375.13, monoclinic, P2 1/c , a = 5.008(3), b = 13.656(13), c = 5.640(3) A, β = 93.04(4)°, V = 385.2 A 3 , Z = 4, Dm = 5.96, Dx = 6.16 Mgm -3 , χ(MoK∝) = 471.5 cm -1 , R = 0.156, Rw = 0.161. Manganese is octahedrally coordinated by fluorine atoms. The octahedra share cis-fluorine atoms to give [MnF sol4 1 F sol2 2 ] infinite chains. The octahedra are Jahn-Teller distorted with the Mn-F bnod distances of 2.10(3) and 2.16(4) A in the directino of the distortion, the other Mn-F bond distances are in the range from 1.84(4) A. The lead atoms are surrounded by eleven fluorine atoms, contact distances are in the range from 2.27(3) to 3.35(4) A. The Madelung Part of Lattice Energy, MAPLE, as well as Effective Coordination Numbers, ECoN, are calculated and discussed." @default.
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- W2016104013 date "1989-10-01" @default.
- W2016104013 modified "2023-10-15" @default.
- W2016104013 title "Synthesis and crystal structure of lead pentafluoromanganate (III), PbMnF5" @default.
- W2016104013 doi "https://doi.org/10.1016/s0022-1139(00)84444-9" @default.
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