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• W2016116616 abstract "Abstract This work reports on the preparation of cellular-like Co 3 O 4 nanocrystals with tailored physical properties via a seeded method by high temperature disposal. By increasing the disposal temperature, Co(OH) 2 seeds can be efficiently transformed to Co 3 O 4 nanocrystals. Systematic sample characterization using combined techniques of X-ray diffraction, scan electron microscope, Fourier transformed infrared spectra, UV–visible diffuse reflectance spectra, Barrett–Emmett–Teller technique and XPS spectra indicates that Co 3 O 4 nanocrystals showed a monotonically lattice expansion with particle size reduction, which can be well-defined as a function of particle sizes as well as valence state of cobalt ions. As the consequence of lattice expansion of Co 3 O 4 nanocrystals, the ν 1 and ν 2 modes of Co 3 O 4 in infrared spectra showed systematic red shift from 580, 669 to 568, 663 cm −1 , respectively. Co 3 O 4 nanocrystals prepared at 300 °C displayed highest catalytic property for HCHO conversion, which can be explained by the balance of surface absorbed OH groups, BET surface area and charge state of cobalt ions." @default.
• W2016116616 created "2016-06-24" @default.
• W2016116616 creator A5002096737 @default.
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• W2016116616 date "2013-03-01" @default.
• W2016116616 modified "2023-09-27" @default.
• W2016116616 title "Synthesis of cellular-like Co3O4 nanocrystals with controlled structural, electronic and catalytic properties" @default.
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• W2016116616 doi "https://doi.org/10.1016/j.jallcom.2012.10.164" @default.
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