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• W2016120437 abstract "A new kinetic method is developed for the determination of hydroperoxyl radical (HO(2)(*))/superoxide radical (O(2)(*)(-)) in aqueous solution, and the calibration using a kinetic half-life technique is also established for determining the concentration of HO(2)(*)/O(2)(*)(-) as produced in the UV/H(2)O(2) process. This new method is based on the reduction of Fe(3+)-EDTA into Fe(2+)-EDTA by HO(2)(*)/O(2)(*)(-) and the well-known Fenton-like reaction of H(2)O(2) and Fe(2+)-EDTA to yield the hydroxyl radicals (OH(*)). Benzoic acid scavenges the OH radicals to produce hydroxybenzoic acids, which are analyzed by fluorescence detection (lambda(ex) = 320 nm; lambda(em) = 400 nm). The limit of detection for the new method depends on the pH values, and it is determined as 3.22 x 10(-)(11) M with signal-to-noise ratio of 2 at pH 5. In addition, the present technique has the advantage of using inexpensive and easily available nonenzymatic reagents that do not require the specific instrument and chemicals and of being insensitive to the moderate concentration of possible interferences often found in aqueous phase." @default.
• W2016120437 created "2016-06-24" @default.
• W2016120437 creator A5022785823 @default.
• W2016120437 creator A5033481196 @default.
• W2016120437 date "2004-10-01" @default.
• W2016120437 modified "2023-10-02" @default.
• W2016120437 title "A Kinetic Method for HO₂^•/O₂^•^- Determination in Advanced Oxidation Processes" @default.
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• W2016120437 doi "https://doi.org/10.1021/ac0493828" @default.
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