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• W2016121063 abstract "Abstract Reaction of [Cp*Fe(CO) 2 I] (Cp* = η 5 ‐C 5 Me 5 ) with an excess amount of BH 3 · thf in toluene at 75 °C or with LiBH 4 at –78 °C leads to the isolation of hydrogen‐rich ferraborane arachno ‐[Cp*Fe(CO)B 3 H 8 ] in good yield. In a similar fashion, reaction of [Cp*M(CO) 3 Cl] (M = Mo and W) with an excess amount of BH 3 · thf at 80 °C or at –78 °C with LiBH 4 yielded metallaboranes [(Cp*M) 2 B 5 H 9 ] (M = Mo, W). Isolated yields of closo ‐[(Cp*M) 2 B 5 H 9 ], (M = Mo and W), both from LiBH 4 and BH 3 · thf, are good. All compounds were characterized in solution by IR, 1 H, 11 B, and 13 C NMR spectroscopy and mass spectrometry and the structural types were unequivocallyestablished by crystallographic analysis of arachno ‐[Cp*Fe(CO)B 3 H 8 ].(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2009)" @default.
• W2016121063 created "2016-06-24" @default.
• W2016121063 creator A5000549665 @default.
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• W2016121063 creator A5067129564 @default.
• W2016121063 creator A5075230954 @default.
• W2016121063 date "2009-03-30" @default.
• W2016121063 modified "2023-10-17" @default.
• W2016121063 title "An Efficient Route to Group 6 and 8 Metallaborane Compounds: Synthesis of <i>arachno</i>‐[Cp*Fe(CO)B₃H₈] and <i>closo</i>‐[(Cp*M)₂B₅H₉] (M = Mo, W)" @default.
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• W2016121063 doi "https://doi.org/10.1002/ejic.200801137" @default.
• W2016121063 hasPublicationYear "2009" @default.
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