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• W2016128076 abstract "Trans-dihydroxo-[tetrakis(2,6-dichlorophenyl)porphinato]ruthenium(IV) ([Ru(OH)2(TDCPP)]) was prepared by meta-chloroperbenzoic acid oxidation of [Ru(CO)(TDCPP)] in dichloromethane-toluene, and its crystal structure is reported. Crystal data for [Ru(OH)2(TDCPP)]·2toluene:C44H22N4O2Cl8Ru·2C7H8, orthorhombic, space group Pbca a = 13.149(1), b = 19.893(2), c = 21.093(2)Å, U = 55.17.3(2) Å3, Z = 4. The short axial RuO bond distance, 1.790(7) Å, is in the range expected for a double Ru(IV)-oxygen bond. Both hydroxo ligands are approximately located in the mean plane of two opposite dichlorophenyl groups. Full-matrix least-squares refinement of positional and thermal parameters, using 2368 unique reflections with F > 2.5 σ (F) led to R(F) = 0.063; Rw = 0.066." @default.
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• W2016128076 date "1995-12-01" @default.
• W2016128076 modified "2023-10-17" @default.
• W2016128076 title "Preparation and crystal structure of trans-dihydroxo-[tetrakis(2,6-dichlorophenyl)porphinato]ruthenium(IV)·2toluene" @default.
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• W2016128076 doi "https://doi.org/10.1016/0020-1693(95)04523-6" @default.
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