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• W2016180546 abstract "Abstract Li 4 Ti 5 O 12 /carbon (LTO/C) nanocomposites are synthesized by preparing surface-modified LTO nanoparticles in supercritical methanol and subsequently calcinating the modified LTO under an Ar/H 2 condition. The effects of surface modifiers with different functional groups and chain lengths (oleylamine, oleic acid, hexylamine) on the particle morphology, particle size, crystallinity, carbon structure, and electrochemical properties are examined. During heat treatment at 750 °C, the carbonization of the modifiers attached to the surface of LTO effectively inhibit the particle growth and reduce some of the Ti 4+ in LTO to Ti 3+ . A higher degree of surface modification, in the order of oleylamine > hexylamine > oleic acid, results in a higher carbon content, smaller particle size, and higher Ti 3+ content; these factors may result in better battery performance of the LTO/C synthesized using oleylamine. At a low rate of 0.1 C, the LTO/C samples synthesized using the different surface modifiers exhibit similar discharge capacities of 175 mA h/g (which approaches the theoretical capacity of LTO), while at a high rate of 10 C, the discharge capacities are in the order of oleylamine (147.1 mA h/g) > hexylamine (124.2 mA h/g) > oleic acid (101.5 mA h/g). The LTO/C nanocomposites prepared using the three different surface modifiers exhibit excellent cyclability up to 200 cycles at 1.0 C." @default.
• W2016180546 created "2016-06-24" @default.
• W2016180546 creator A5010132153 @default.
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• W2016180546 date "2015-06-01" @default.
• W2016180546 modified "2023-09-27" @default.
• W2016180546 title "Synthesis of Li4Ti5O12/carbon nanocomposites in supercritical methanol for anode in Li-ion batteries: Effect of surface modifiers" @default.
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• W2016180546 doi "https://doi.org/10.1016/j.supflu.2015.03.001" @default.
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