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• W2016203970 abstract "O-Benzylation of the flexible macrocycle 1 with benzyl bromide in the presence of NaH in THF under reflux afforded a mixture of two conformers of the tri-O-benzylated products, cone-2a and partial-cone-2a in a ratio of 20∶80 in 80% yield. In contrast, O-alkylation of the triol 1 with 2-(chloromethyl)pyridine in the presence of NaH resulted in exclusive formation of cone-2b. Only when the template metal can hold the 2-pyridyl group(s) and the oxide group(s) on the same side of the [3.3.3]metacyclophane ring, is the conformation immobilized in the cone form. The template effect of the sodium cation plays an important role in this benzylation." @default.
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• W2016203970 date "1998-01-01" @default.
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• W2016203970 title "Synthesis, conformational studies and inclusion properties of O-benzylated calixarene analogues of trihydroxy[3.3.3]metacyclophanes" @default.
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• W2016203970 doi "https://doi.org/10.1039/a704064d" @default.
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