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• W2016205211 startingPage "807" @default.
• W2016205211 abstract "Effects of sterilization by electron beam (E-BEAM) on paclitaxel (1) mixed with poly(DL-lactide-co-glycolide) (PLG) in reservoirs of COSTAR Stents are examined by using liquid chromatography-mass spectrometry (LC-MS-MS) techniques with information-dependent acquisition (IDA). Numerous degradation products of 1 are formed in a β-radiation dose-dependent manner to give plethora of low-level degradants. This behavior, together with multiple interferences from PLG-related compounds, creates considerable challenges for analysis of the drug/PLG mixtures. IDA methods with different survey scans are proven to be very efficient in elucidating degradation pathways and in identifying numerous products. Combined LC-MS-MS results from analysis of sterilized drug substance and stents indicate that water addition and oxidative processes together with the isomerization are largely responsible for degradation of 1 under E-BEAM sterilization conditions used." @default.
• W2016205211 created "2016-06-24" @default.
• W2016205211 creator A5045329663 @default.
• W2016205211 creator A5090444369 @default.
• W2016205211 date "2011-11-01" @default.
• W2016205211 modified "2023-09-25" @default.
• W2016205211 title "Effects of E-BEAM Sterilization on Drug-Eluting Stents: Paclitaxel Degradation Elucidated by LC-MS-MS with Information-Dependent Acquisition" @default.
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• W2016205211 doi "https://doi.org/10.1093/chrsci/49.10.807" @default.
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