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• W2016291933 abstract "Single-crystalline sulfated c-ZrO2(111) films of the cubic (c) type have been prepared by reactive deposition of Zr onto Pt(111) in an O2 atmosphere and subsequent exposition to a SO3 atmosphere. The morphology, atomic structure, and composition have been examined by scanning tunneling microscopy, low-energy electron diffraction (LEED), Auger electron spectroscopy, and density functional theory (DFT) calculations. The clean c-ZrO2(111) films display a (2 × 2) surface structure. During SO3 exposure at room temperature, a clear (√3 × √3)R30° structure develops. At about 700 K, the SO3-induced (√3 × √3)R30° structure disappears and the bright (2 × 2) LEED pattern of the clean ZrO2 films reappears. The energies of plausible c-ZrO2(111)/SO3 structures have been examined by DFT. The (√3 × √3)R30° structure found in the experiments turned out to be the most stable one for temperatures below 700 K. At temperatures around 700 K, a disordered low coverage structure may exist, which can not be observed by conventional LEED. A comparison of cubic zirconia surfaces with the alternative tetragonal system yields similar results for the SO3 adsorption in the DFT calculations and shows that c-ZrO2 surfaces are good models for the industrial used tetragonal ZrO2 supports." @default.
• W2016291933 created "2016-06-24" @default.
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• W2016291933 date "2006-01-01" @default.
• W2016291933 modified "2023-09-27" @default.
• W2016291933 title "Interaction of SO3 with c-ZrO2(111) films on Pt(111)" @default.
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• W2016291933 doi "https://doi.org/10.1039/b516190h" @default.
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