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- W2016408834 abstract "The chiral lactam 1 (or its enantiomer ent-1) was shown to be an effective (1)H NMR shift reagent for the ee determination of chiral lactams, quinolones, and oxazolidinones. It was successfully employed in many cases in which a detection of enantiomers by chromatographic methods failed. The method was extended to a broader range of simple substrates bearing a lactam moiety to evaluate its scope. The NH signals of the substrate enantiomers showed the strongest separation and were used for (1)H NMR integration. In most cases, compound 1 (1.5 equiv; 0.06 M solution) induced a baseline separation of the NH signals and it can consequently be regarded as a generally applicable shift reagent for chiral products with a lactam moiety." @default.
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- W2016408834 date "2004-01-14" @default.
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- W2016408834 title "An Enantiomerically Pure 1,5,7-Trimethyl-3-azabicyclo[3.3.1]nonan- 2-one as <sup>1</sup>H NMR Shift Reagent for the <i>e</i><i>e</i> Determination of Chiral Lactams, Quinolones, and Oxazolidinones" @default.
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- W2016408834 doi "https://doi.org/10.1021/jo0354847" @default.
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