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• W2016452704 abstract "A novel approach was developed for nitrate analysis in a FIA configuration with amperometric detection (E = −0.48 V). Sensitive and reproducible current measurements were achieved by using a copper electrode activated with a controlled potential protocol. The response of the FIA amperometric method was linear over the range from 0.1 to 2.5 mmol L−1 nitrate with a detection limit of 4.2 μmol L−1 (S/N = 3). The repeatability of measurements was determined as 4.7% (n = 9) at the best conditions (flow rate: 3.0 mL min−1, sample volume: 150 μL and nitrate concentration: 0.5 mmol L−1) with a sampling rate of 60 samples h−1. The method was employed for the determination of nitrate in mineral water and soft drink samples and the results were in agreement with those obtained by using a recommended procedure. Studies towards a selective monitoring of nitrite were also performed in samples containing nitrate by carrying out measurements at a less negative potential (−0.20 V)." @default.
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• W2016452704 date "2009-12-01" @default.
• W2016452704 modified "2023-10-07" @default.
• W2016452704 title "A renewable copper electrode as an amperometric flow detector for nitrate determination in mineral water and soft drink samples" @default.
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• W2016452704 doi "https://doi.org/10.1016/j.talanta.2009.07.028" @default.
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