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• W2016483623 abstract "Abstract Ta x Ti 1− x C and Ta x Ti 1− x C y N 1− y (0 ≤  x  ≤ 1, 0 ≤  y  ≤ 1) whiskers have been oxidised under non-isothermal as well as isothermal conditions. The non-isothermal oxidation experiments were carried out in a combined thermogravimetric – differential thermal analysis set-up (TG-DTA), using oxygen atmosphere, with a heating rate of 5°C/min. It was found that the oxidation onset temperature ( T on ) increased with increasing x -value within the temperature range 375–550°C for both Ta x Ti 1− x C and Ta x Ti 1− x C y N 1− y whiskers and also that T on is higher for carbonitrides compared to carbides. Scanning and transmission electron microscopy studies (SEM and TEM) showed that whiskers with a diameter exceeding 0.3 μm were split into two halves along the length of the whisker when oxidised, whereas whiskers with a diameter less than 0.3 μm retained their morphology after oxidation. Isothermal oxidation experiments were performed with Ta x Ti 1− x C whiskers in the temperature range 400–1200°C, and it was found that the size of TiO 2 particles formed from mixed transition-metal carbide precursors was substantially smaller compared to the particle size resulting from oxidation of TiC. However, the size of Ta 2 O 5 particles were found to be small and of the same size independently if TaC or Ta x Ti 1− x C were oxidised." @default.
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• W2016483623 date "1999-09-01" @default.
• W2016483623 modified "2023-09-27" @default.
• W2016483623 title "Oxidation behaviour of TaxTi1−xC and TaxTi1−xCyN1−y whiskers" @default.
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• W2016483623 doi "https://doi.org/10.1016/s0040-6031(99)00214-2" @default.
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