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• W2016550183 abstract "The new mineral argesite, ammonium bismuth chloride (NH4)7Bi3Cl16, was found in a mediumtemperature (~250 °C) active fumarole at La Fossa crater, Vulcano, Aeolian Islands, Sicily, Italy. The mineral occurs on a pyroclastic breccia as pale-yellow crystals up to 0.15 mm in length, in association with bismuthinite, adranosite, brontesite, demicheleite-(Br), demicheleite-(Cl), and panichiite. Argesite is trigonal, space group: R3̅c (no. 167) with Z = 18; the unit-cell parameters are (single-crystal data): a = 13.093(1), c = 102.682(1) Å, and V = 15245(2) Å3. The six strongest reflections in the X-ray powder diffraction pattern are: [dobs(Å) (I) (hkl)] 3.164 (100) (0 3 18), 3.808 (44) (2̅ 2 20), 2.742 (78) (2̅ 4 21), 6.14 (16) (1̅ 2 6), 1.906 (16) (0 0 5̅4̅), 1.686 (13) (5̅ 6 34). The mineral is uniaxial (-), with ω = 1.731(2), ε = 1.725(2) (589 nm). The IR spectrum shows absorptions at 3188(vs), 3060(s), and 1397(vs) cm-1, in agreement with the presence of the ammonium ion. Chemical analyses obtained by EDS electron microprobe gave (average wt%) Bi 42.26, Cl 32.57, Br 13.06, I 0.95, K 2.46, Tl 0.88, NH4 7.82 (by difference) total 100.00, corresponding to the empirical formula: [(NH4)6.29K0.91Tl0.06]Σ7.26Bi2.93(Cl13.33Br2.37I0.11)Σ15.81. The measured density is 2.88(1) g/cm3. The structure was refined, using single-crystal diffraction data, to a final R = 0.0345 for 1289 independent observed reflections [I > 2σ(I)]. It contains Bi2Cl4-10 and BiCl3-6 anions where the Bi atoms are octahedrally coordinated, and NH+4 cations are partially replaced by K+ and Tl+ ions." @default.
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• W2016550183 date "2012-08-01" @default.
• W2016550183 modified "2023-10-12" @default.
• W2016550183 title "Argesite, (NH4)7Bi3Cl16, a new mineral from La Fossa Crater, Vulcano, Aeolian Islands, Italy: A first example of the [Bi2Cl10]4- anion" @default.
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• W2016550183 doi "https://doi.org/10.2138/am.2012.4052" @default.
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