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- W2016662370 abstract "Abstract Photochemical formation of α-hydroxycyclic nitrone from the nitrite of a fused 5-membered ring alcohol is described. The nitrite (VI) of N-acetyl-22,27-imino-12α-jerv-4, 13(17)-dien-11β-ol-3,23-dione was prepared from jervine and photolyzed under the conditions of the Barton reaction to afford a single rearranged product VII. The structure of VII was established as a cyclic nitrone (VII) on the basis of the Mass, IR, UV, NMR spectroscopy, chemical and photochemical evidence and the consideration of the mode of the formation. The reaction is unprecedented. The unusual formation of oxaziridine (XIa, XIb) and pyridine nucleus (XII) from hydroxynitrone (VII) under the condition of acylation has been found." @default.
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- W2016662370 date "1971-01-01" @default.
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- W2016662370 title "Photochemical formation of cyclic nitrone from nitrite of a fused 5-membered ring alcohol" @default.
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- W2016662370 doi "https://doi.org/10.1016/s0040-4020(01)98192-x" @default.
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