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- W2016678297 abstract "Because of the occurrence of ion exchange between high-ionic-strength solution and anions of polymeric ionic liquids (PILs), PILs based solid-phase microextraction (SPME) fibers were rarely used in direct immersion mode to high-salt-added samples. In this work, a novel double-confined PIL sorbent was prepared by co-polymerization of cation and anion of 1-vinyl-3-octylimidzaolium p-styrenesulfonate (VOIm+SS−). The poly(VOIm+-SS−) was chemically bonded onto functionalized stainless steel wire via surface radical chain-transfer reaction. Stability of poly(VOIm+-SS−) in high-ionic-strength solution was investigated and compared with that of poly(1-vinyl-3-octylimidzaolium benzenesulfonate) (poly(VOIm+BS−)) by elemental analysis of sulfur element, and results turned out that the poly(VOIm+-SS−) was more stable. Coupled to gas chromatography (GC), the poly(VOIm+-SS−) fiber was used to extract three sorts of compounds including anilines, phenols and phthalate esters in aqueous solution. The as-established method showed good linearity, low detection limits, and acceptable repeatability. The direct immersion SPME-GC method was applied to determine the model phthalate esters in bottled mineral water. The determination results were satisfactory." @default.
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- W2016678297 date "2012-12-01" @default.
- W2016678297 modified "2023-10-07" @default.
- W2016678297 title "Novel double-confined polymeric ionic liquids as sorbents for solid-phase microextraction with enhanced stability and durability in high-ionic-strength solution" @default.
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- W2016678297 doi "https://doi.org/10.1016/j.chroma.2012.10.037" @default.
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