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- W2016684360 abstract "Interaction of M(CO)6 (M=Cr, Mo, W) with 4-phenylpyridin (L) under photolytic conditions leads to the formation of L·M(CO)5. The reaction of 2,6-diphenylpyridine (C17H13N) with hexacarbonyl chromium in boiling dibutyl ether yields C17H13N·Cr(CO)3 and C17H13N·2Cr(CO)3. Analogously 2,4,6-triphenylpyridine (C23H17N) and hexacarbonyl chromium give C23H17N·Cr(CO)3, C23H17N·2Cr(CO3 and C23H17N·3Cr(CO)3. IR, NMR, UV and mass spectra of these complexes are reported. The proton NMR spectra indicate that the Cr(CO)3 groups are bonded to the phenyl substituents and not to the central pyridine ring. Die Einwirkung von M(CO)6 (M=Cr, Mo, W) auf 4-Phenylpyridin (L) führt unter photolytischen Bedingungen zu L·M(CO)5. Die Umsetzung von 2,6-Diphenylpyridin (C17H13N) mit Chromhexacarbonyl in siedendem Dibutyläther ergibt C17H13N·Cr(Co)3 und C17H13N·2Cr(CO)3. Analog liefern 2,4,6-Triphenylpyridin (C23H17N) und Chromhexacarbonyl C23H17N·Cr(CO)3, C23H17N·2Cr(CO)3 und C23H17N·3Cr(CO)3. Es wird über die IR-, NMR-, UV- und Massenspektren dieser Komplexe berichtet. Die Protonenresonanzspektren zeigen, dass die Cr(CO)3-Gruppen an die Phenylsubstituenten und nicht an den zentralen Pyridinring gebunden sind." @default.
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- W2016684360 title "Über chromcarbonylkomplexe phenylsubstituierter pyridine" @default.
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- W2016684360 doi "https://doi.org/10.1016/s0022-328x(00)86556-0" @default.
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