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- W2016886838 abstract "The only reported preparation of a hexakis(dialkylamino)disilane, namely, (Me 2 N) 3 SiSi(NMe 2 ) 3 (1) was stated to proceed quantitatively. In our hands, this preparation repeatedly gave a mixture only ∼40% and ∼60% of the new compound (Me 2 N) 3 SiSi(NMe 2 ) 2 Cl(2). Compound 1 was made in 84% yield, however, by treating the aforementioned mixture with LiNMe 2 in THF, and 2 can be prepared in 91% yield from Si 2 Cl 6 and excess HNMe 2 using ether as the solvent." @default.
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- W2016886838 date "2010-08-20" @default.
- W2016886838 modified "2023-09-25" @default.
- W2016886838 title "ChemInform Abstract: Synthesis of (Dialkylamino)disilanes." @default.
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- W2016886838 doi "https://doi.org/10.1002/chin.199322218" @default.
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