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- W2016908241 abstract "The crystal structure of Pr2(S2O6)3(Ph3PO)6(H2O)6 (1), has been determined and is compared with the previously reported Nd2(S2O6)3(Ph3PO)4(H2O)8 (2), and Nd2(S2O6)3·14H2O (3). The steric congestion in the primary coordination sphere, evaluated by steric angle sum (SAS) calculations, shows that all the complexes have SAS values within the expected range for the coordination number of the metal. The incorporation of extra Ph3PO in 1 is accommodated by a very long PrOH2 distance. The behaviour of lanthanide dithionates and their triphenylphosphine oxide complexes under electrospray mass spectrometry conditions has been investigated. For Ln2(S2O6)3, the expected ions, Ln(S2O6)+ and Ln(S2O6)2−, and their methanol solvates, are observed as weak signals. The relationship between these and the major ions observed in the gas phase is discussed. The spectra of the triphenylphosphine oxide complexes show no lanthanide containing ions." @default.
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- W2016908241 title "Complexes of lanthanide dithionates 2. Electrospray mass spectrometry of Ln2(S2O6)3 and their Ph3PO complexes; the X-ray crystal structure of Pr2(S2O6)3(Ph3PO)6(H2O)6" @default.
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- W2016908241 doi "https://doi.org/10.1016/s0020-1693(99)00344-8" @default.
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