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- W2016933759 abstract "This paper describes the optimisation and validation of an ultra performance liquid chromatography- tandem mass spectrometry (UPLC-MS/MS) method for the analysis of four pharmaceuticals (flubendazole, pipamperone, rabeprazole and domperidone) and one pesticide (propiconazole) in surface water. Sample preparation was reduced substantially as compared to a previously published high performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) method, thanks to the use of UPLC. In addition, internal standards could now be used for quantification instead of the standard addition method. Extraction was performed on a Speedisk phenyl solid-phase extraction tube. A Waters Acquity HSS T3 UPLC column (100 × 2.1 mm i.d.; 1.8-µm particles) was used for separation and an API 4000 triple quadrupole was used as a detector. Total run time was 8.59 minutes. Matrix effects were examined on different surface water samples. Limits of detection and quantification in surface water samples were between 100 and 500 pg/l. Validation was performed on surface water. The method showed good precision (<15%) and accuracy (85–120%). This method is less time-consuming and labour-intensive than a previously published HPLC-procedure without compromising validation parameters." @default.
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- W2016933759 date "2011-10-01" @default.
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- W2016933759 title "Determination of four basic pharmaceuticals and one pesticide in surface water with UPLC-ESI-MS/MS" @default.
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- W2016933759 doi "https://doi.org/10.1080/03067311003778664" @default.
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