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• W2017013671 abstract "The effect of various benzenesulfonamide (BSA) plasticizers on the amorphous phase of semicrystalline polydodecamide (PA-12) has been investigated. MonoBSAs appear as efficient glass-transition temperature (Tg) depressors because of their miscibility with the host polyamide (PA), low glass transition, and small molecule size. PA-12's Tg shifts from 50 to about 0 °C at 20 mol % of the most efficient molecules. Comparatively, the more bulky bisBSAs appear to induce less important absolute Tg decreases (30 K at 20 mol %), although these appear as more important when considering the polymer Tg to plasticizer Tg difference. This unexpected observation could be ascribed to both the amide-sulfonamide interactions and the sterically generated disorder within the polyamide because of the plasticizer molecule's size. Phase-separation behavior of BSA plasticizers within the host PA has also been investigated. Crystalline phenyl-SO2NH2, for instance, dephased beyond 20 mol % in PA-12, forming distinct 1–2 micrometer wide crystalline domains as a result of its high propensity to crystallize upon cooling from the melt. By contrast, slow crystallizing N,N-dimethylBSA, which lacks any specific interaction for PA-12, remained nevertheless dispersed at a molecular level (metastable state, no phase separation) when vitrification of the host PA-12 amorphous phase occurred on cooling. © 2002 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 40: 2208–2218, 2002" @default.
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• W2017013671 date "2002-08-22" @default.
• W2017013671 modified "2023-09-26" @default.
• W2017013671 title "Effect of benzenesulfonamide plasticizers on the glass-transition temperature of semicrystalline polydodecamide" @default.
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• W2017013671 doi "https://doi.org/10.1002/polb.10281" @default.
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