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- W2017016961 abstract "A solid sorbent technique was developed to measure volatile halogenated organic compounds (VHOCs) in soil gas. The VHOCs were preconcentrated onto graphitized carbon black (Carbotrap) and analyzed by thermal desorption/high-resolution gas chromatography with electron-capture detection. The method detection limit (MDL) for trichloromethane (CHCl3) and tetrachloromethane (CCl4) in soil gas was approximately 1 μg m−3 for a 60-ml sample volume. A thermal-desorption temperature of 200°C was sufficient to recover more than 90% of the VHOCs from the sorbent. Breakthrough volumes for CHCl3 and CCl4 were at least 1000 ml when soil gas was drawn through the sample cartridge at a rate of 30 ml min−1. Sorbent cartridges stored at 20°C were sufficiently stable for at least 30 days. Application of the method in the field indicated that the measured concentration of VHOCs in soil-gas monitoring wells was sensitive to the volume of soil gas that was withdrawn." @default.
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- W2017016961 title "Solid sorbent method for the collection and analysis of volatile halogenated organic compounds in soil gas" @default.
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