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- W2017046935 abstract "Abstract The sodium or potassium salt of 4-vinyl benzenesulphonic acid was epoxidized conveniently by 3-chloroperoxybenzoic acid. Several solvent systems for the reaction were investigated and it was found that a water/ethanol mixture was most efficient at room or elevated temperatures. The epoxide formed was relatively stable and was isolated and analysed by n.m.r. and i.r., Ring opening of the epoxide with sodium carbonate resulted in the production of the diol, potassium or sodium 4-(1,2-dihydroxyethyl) benzenesulphonate, in good yield. The new ionic diol was incorporated into polyurethane by step-growth solution copolymerization in the presence of di-n-butyltin dilaurate. Proton n.m.r., i.r., t.g.a. and the solubility of the ionomer were investigated." @default.
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- W2017046935 date "1989-12-01" @default.
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- W2017046935 title "Sulphonated polyurethane ionomers with new ionic diols" @default.
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- W2017046935 doi "https://doi.org/10.1016/0032-3861(89)90268-1" @default.
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