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- W2017128541 abstract "Abstract Magnetic nanoparticles of Fe 3 O 4 had been fabricated through hydrothermal reaction by using sodium bis(2-ethylhexyl) sulfosuccinate (AOT) as a surfactant and hydrazine hydrate (N 2 H 4 ·H 2 O) as a reductant. The influences of different concentrations of AOT and N 2 H 4 ·H 2 O on the nanoparticles were investigated; moreover, the different reaction temperatures and time were also analyzed. Their structure and morphology were characterized by X-ray powder diffraction (XRD), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), energy dispersive spectrometer (EDS) and Fourier transform infrared spectroscopy (FT-IR). Furthermore, magnetic properties of the products were studied by vibrating sample magnetometer (VSM). The crystallite size of the samples was calculated using Debye–Scherrer equation. It was found that the as-prepared nanoparticles had been modified by using surfactant during the synthesis process. The amount of AOT and N 2 H 4 ·H 2 O, the reaction temperature and time had effects on the size, the dispersal and the magnetic properties of the particles. The well-dispersed magnetic Fe 3 O 4 nanoparticles with better size distribution could be prepared at 150 °C for 10 h when the concentrations of AOT and N 2 H 4 ·H 2 O were 0.10 M and 20% (v/v), respectively. Besides, possible mechanisms related to the effects were also discussed." @default.
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- W2017128541 date "2009-01-01" @default.
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- W2017128541 title "Influences of different synthesis conditions on properties of Fe3O4 nanoparticles" @default.
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- W2017128541 doi "https://doi.org/10.1016/j.matchemphys.2008.06.036" @default.
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