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- W2017148963 abstract "The influence of the inner capillary diameter, length of the capillary, linear velocity of the mobile phase and volume of the retentive liquid segment on the dynamic range of the gradient and the efficiency of enrichment of the new preconcentration technique was studied. Phenol, 2,4-dinitroaniline, phenanthrene and fluoranthene in water solution were used as model analytes. Capillaries with inner diameters of 0.095 mm and 0.2 mm and lengths ranging from 3.5 to 15 m were examined. The segment of the retentive liquid in capillary was generated by the injection of suitable volume of cyclohexanol. It was found that the enrichment increases with decrease in the inner capillary diameter and with increase in its length. The working range of this technique was found. With analytes in sub-ppb concentrations in the injected sample, an enrichment factor up to 280 was achieved. The application possibilities of proposed procedure was demonstrated by off-line capillary GC analysis of collected enriched solution of model mixtures of alkyl phthalates and polyaromates." @default.
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- W2017148963 date "1997-12-01" @default.
- W2017148963 modified "2023-10-02" @default.
- W2017148963 title "Influence of the capillary dimensions on the performance of the preconcentration technique based on parallel current chromatography" @default.
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- W2017148963 doi "https://doi.org/10.1016/s0021-9673(97)00772-3" @default.
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