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- W2017226783 abstract "Abstract The previously described α-Burke 1 chiral stationary phase (CSP) was designed for the chromatographic separation of the enantiomers of s-blockers. Difficulties with the reproducibility of the free radical addition reaction, used in the attachment of the chiral selector to the chromatographic support, have required the development of an alternative silane immobilization process (α-Burke 2 CSP). While the enantioselectivity afforded by this new CSP is generally equivalent to that of the original CSP, the α-Burke 2 CSP demonstrates longer analyte retention, necessitating the use of mobile phases of greater eluotropic strength. The increased retention of the new CSP presumably results from a greater surface density of functional selectors, an interpretation which is supported by the observation that the preparative capacity of the α-Burke 2 CSP is greater than that of the original. Some of the factors influencing the retention and separation of a group of 23 s-blockers on the α-Burke 2 CSP are discussed." @default.
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- W2017226783 title "Improved chiral stationary phase for ß-blocker enantioseparations" @default.
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