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- W2017231310 abstract "A highly specific and sensitive GLC method was developed for the analysis of alpha,alpha-dimethyl-4-(alpha,alpha,beta,beta-tetrafluorophenethyl) benzylamine, a new orally active antiarrhythmic drug, in biological fluids. The procedure involves the addition of an internal standard, 4-(alpha,alpha,beta,beta-tetrafluorophenethyl)benzylamine, to the plasma or urine samples followed by extraction of the drugs into benzene at pH 8. The extracted amines are converted to the trifluoroacetyl derivatives (characterized by GLG-mass spectrometry), chromatographed, and detected with a 63Ni electron-capture detector. The sensitivity of the method is such that 10 ng of alpha,alpha-dimethyl-4-(alpha,alpha,beta,beta-tetrafluorophenethyl)benzylamine/ml of plasma can be analyzed. These levels are suitable for the analysis of samples obtained following a therapeutic dose." @default.
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- W2017231310 modified "2023-09-25" @default.
- W2017231310 title "Electron-Capture GLC Determination of a New Antiarrhythmic Agent, α,α-Dimethyl-4-(α,α,β,β-tetrafluorophenethyl)benzylamine, in Biological Fluids" @default.
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- W2017231310 doi "https://doi.org/10.1002/jps.2600640518" @default.
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