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• W2017264944 abstract "A novel bicyclic bis(γ-butyrolactone), 2,8-dioxa-1-isopropenylbicyclo[3.3.0]octane-3,7-dione (2), was successfully synthesized by the reaction of 1,2,3-propanetricarboxylic acid and methacrylic anhydride at 140 °C in the presence of N,N-dimethyl-4-aminopyridine and CuCl2. Anionic ring-opening copolymerization of 2 with glycidyl phenyl ether (GPE) using PPh3 as an initiator proceeded in a 1:1 alternating manner to give the corresponding polyester 3 bearing α,β-unsaturated ketone groups in the side chains. Prolongation of polymerization time resulted in the production of an insoluble networked copolymer due to reactions of the α,β-unsaturated ketone groups in the side chains. In order to demonstrate the potential of the copolymer 3 as a reactive polymer, Michael addition of thiols to the α,β-unsaturated ketone groups in the side chains was performed." @default.
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• W2017264944 date "2011-03-04" @default.
• W2017264944 modified "2023-10-14" @default.
• W2017264944 title "Synthesis of a Reactive Polyester Bearing α,β-Unsaturated Ketone Groups by Anionic Alternating Copolymerization of Epoxide and Bicyclic Bis(γ-butyrolactone) Bearing Isopropenyl Group" @default.
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• W2017264944 doi "https://doi.org/10.1021/ma102602e" @default.
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