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• W2017289985 abstract "The effect of mechanical activation on formation of calcium titanate (CaTiO3) from calcined mixtures of CaCO3 and TiO2 was studied by monitoring the course of this solid-state reaction by variable temperature in situ X-ray diffraction (XRD) experiments, scanning electron microscopy (SEM) and dilatometry. Two equimolar mixtures of powdered CaCO3 and TiO2 were prepared: one was mechanically activated by grinding in a high energy vibro-mill. A total of 32 X-ray diffraction data sets for each sample, collected between 30 and 1100 °C, were analyzed by multiphase Rietveld refinement. Quantitative phase analysis and microstructure analysis obtained from X-ray diffraction are correlated to results of scanning electron microscopy and dilatometry. In the non-activated sample, small quantities of the reactants remain in the product until 1100 °C. In the activated sample, the reaction results in pure CaTiO3 at 920 °C." @default.
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• W2017289985 date "2003-06-01" @default.
• W2017289985 modified "2023-10-05" @default.
• W2017289985 title "Variable temperature in situ X-ray diffraction study of mechanically activated synthesis of calcium titanate, CaTiO3" @default.
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• W2017289985 doi "https://doi.org/10.1016/s0025-5408(03)00113-2" @default.
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