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- W2017323905 abstract "Abstract We explore the structure directing role of the chiral cation (1S,2S)-2-hydroxymethyl-1-benzyl-1-methylpyrrolidinium (SS-bmpm) in the synthesis of Al-containing zeolite materials in the presence of co-structure directing agents (co-SDAs). Three different co-SDAs are studied: tetramethylammonium (TMA), quinuclidine and sodium. Synthesis with TMA as co-SDA yields a ferrierite related phase and a material from the MWW family, where the SS-bmpm and the TMA cations are incorporated intact within the samples. Quinuclidine produces instead amorphous solids, while the use of Na + leads to crystalline phases that crystallized as a result of the degradation of the SS-bmpm cation. A subsequent computational study based on molecular mechanics was performed in an attempt to unravel the location of TMA and SS-bmpm cations within the void space of the complex MWW structure. The results suggest that the sinusoidal channels are exclusively filled by TMA, while the bulky SS-bmpm cations can only be accommodated within the MWW super-cages, thus providing a new example of cooperative structure-directing effects of small and bulky cations in the synthesis of complex zeolite structures." @default.
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- W2017323905 date "2012-01-01" @default.
- W2017323905 modified "2023-10-18" @default.
- W2017323905 title "Study of the structure directing effect of the chiral cation (1S,2S)-2-hydroxymethyl-1-benzyl-1-methylpyrrolidinium in aluminosilicate preparations in the presence of co-structure directing agents" @default.
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- W2017323905 doi "https://doi.org/10.1016/j.cattod.2011.07.017" @default.
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