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• W2017362010 abstract "This manuscript describes a new protocol for determination of Pa/Th/U in marine sediments. It is based on microwave-assisted digestion and represents an important reduction of working time over conventional hot-plate digestion methods, and the use of HClO4 is avoided. Although Th and U are completely dissolved with a first microwave step, around 40% of 231Pa remains undissolved, and a short hot-plate step with reverse aqua regia is required to achieve total digestion and spike equilibration. Next, the method involves a separation of these elements and a further purification of the Pa fraction using Dowex AG1-X8 resin. Separation with Bio-Rad and Sigma-Aldrich resins was compared; although both perform similarly for Th and U, Pa yields are higher with Bio-Rad. Finally, samples are measured using a Nu instruments multiple collector inductively coupled plasma mass spectrometer (MC-ICPMS). Overall chemical yields range around 50% for Pa, 60% for Th, and 70% for U." @default.
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• W2017362010 date "2009-02-09" @default.
• W2017362010 modified "2023-10-16" @default.
• W2017362010 title "Separation and Measurement of Pa, Th, and U Isotopes in Marine Sediments by Microwave-Assisted Digestion and Multiple Collector Inductively Coupled Plasma Mass Spectrometry" @default.
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• W2017362010 doi "https://doi.org/10.1021/ac802341y" @default.
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