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• W2017364958 abstract "The reaction layers between silicon carbide continuous fibers (Nicalon) and a calcium aluminosilicate glass-ceramic (anorthite composition) matrix in hot-pressed composites have been characterized both structurally and chemically using high-resolution, field-emission scanning transmission electron microscopy. Chemical compositions at 10-nm spacings, with a resolution of ∼5 nm, were collected across the fiber-matrix interface zone. The reaction sequence in the material is silicon carbide (fiber)—carbon (in this case, graphite)—silica-rich glass—anorthite. The composition of the carbon layer is constant across its width; the interfaces between the four phases are planar. This morphology and the chemical gradients observed are consistent with the simple, ‘carbon-condensed’ oxidation displacemetn reaction, SiC + O2→ SiO2+ C, being responsible for interface phase formation in the composites. The planar interfaces indicate that the rate-limiting process in the interface formation reaction is the diffusion of oxygen through the matrix and silica glass layer; a corollary of this conclusion is that the diffusion of silicon through the carbon layer is a relatively faster process." @default.
• W2017364958 created "2016-06-24" @default.
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• W2017364958 date "1990-10-01" @default.
• W2017364958 modified "2023-10-16" @default.
• W2017364958 title "Reaction-Layer Interfaces in SiC-Fiber-Reinforced Glass-Ceramics: A High-Resolution Scanning Transmission Electron Microscopy Analysis" @default.
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• W2017364958 doi "https://doi.org/10.1111/j.1151-2916.1990.tb06694.x" @default.
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