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• W2017394420 abstract "Treatment of the dihalogeno derivatives [{Mo(η-C5Me5)(NO)X(µ-X)}2][X = Cl, (1a); Br, (1b); or I, (1c)] or [Mo(η-C5Me5)(NO)X2(PPh3)][X = Cl, (2a); Br, (2b); or I, (2c)] with Al2Me6 gives the halogenomethyl complexes [{MoMe(η-C5Me5)(NO)(µ-X)}2](3a)–(3c) or [MoMe(η-C5Me5)(NO)X(PPh3)](4a)–(4c) respectively. Dimers (3) react with PPh3 to give monomers (4). Complex (1b) reacts with LiMe to give [MoMe2(η-C5Me5)(NO)](5). Reactions of (1) or (3b) with Tl(C5H5) give the ‘20-electron’ mixed bis(cyclopentadienyl) complexes [Mo(η-C5H5)(η-C5Me5)(NO)Y][Y = Cl, (6a); Br, (6b); I, (6c); or Me, (7)]. The structure of complex (7)(crystal A) has been determined by X-ray diffraction methods. By accident, the structure of the first crystal examined (B) contained (7) and the oxo complex trans-[{Mo(η-C5Me5)O(µ-O)}2](8) in an ordered mixture with a 2:1 molar ratio. Crystal A is orthorhombic, space group Pna21 with Z= 4 in a unit cell of dimensions a= 9.370(4), b= 12.322(5), and c= 13.301 (5)Å. Crystal B is monoclinic, space group P21/a with Z= 4, (7), and 2, (8), in a unit cell of dimensions a= 32.569(9), b= 8.535(4), c= 9.482(5)Å, and β= 93.33(3)°." @default.
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• W2017394420 date "1990-01-01" @default.
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• W2017394420 title "Synthesis of (pentamethylcyclopentadienyl)nitrosylmolybdenum complexes containing halide, methyl, or cyclopentadienyl ligands. Crystal structures of [MoMe(η-C5H5)(η-C5Me5)(NO)] and [{Mo(η-C5Me5)O(µ-O)}2]" @default.
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• W2017394420 doi "https://doi.org/10.1039/dt9900002779" @default.
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