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- W2017441094 abstract "Tetrathiafulvalene (TTF) monolayers covalently bound to oxide-free hydrogen-terminated Si(100) surfaces have been prepared from the hydrosilylation reaction involving a TTF-terminated ethyne derivative. FTIR spectroscopy characterization using similarly modified porous Si(100) substrates revealed the presence of vibration bands assigned to the immobilized TTF rings and the Si–C═C– interfacial bonds. Cyclic voltammetry measurements showed the presence of two reversible one-electron systems ascribed to TTF/TTF.+ and TTF.+/TTF2+ redox couples at ca. 0.40 and 0.75 V vs SCE, respectively, which compare well with the values determined for the electroactive molecule in solution. The amount of immobilized TTF units could be varied in the range from 1.7 × 10–10 to 5.2 × 10–10 mol cm–2 by diluting the TTF-terminated chains with inert n-decenyl chains. The highest coverage obtained for the single-component monolayer is consistent with a densely packed TTF monolayer." @default.
- W2017441094 created "2016-06-24" @default.
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- W2017441094 date "2012-02-07" @default.
- W2017441094 modified "2023-09-26" @default.
- W2017441094 title "Multiredox Tetrathiafulvalene-Modified Oxide-Free Hydrogen-Terminated Si(100) Surfaces" @default.
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- W2017441094 doi "https://doi.org/10.1021/la204375a" @default.
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