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• W2017460829 abstract "The surface chemistry and structure of nanosized silicon, as obtained by high-energy ball milling and its subsequent dispersion in ethanol, via sonication-assisted oxidation, is presently described. These Si/SiOx suspensions that spontaneously assemble on glass surfaces were investigated as a function of pH in a variety of oxidizing agents and atmospheres. Spectroscopic characterization indicates that at pH 5 or below and in the absence of H2O, the Si−OEt groups present on the surface of these nanoparticles get protonated, providing the driving force to assemble on less positively charged glass substrates. X-ray photoelectron spectroscopy concurs with a core/shell (Si/SiOx) nanoparticle structure, with an average Si-atom ratio of 45/55 and x in the order of 1.5. In addition, Raman investigation suggests that the Si core in these nanoparticles (45% of the total Si-atom content) is composed of crystalline (34%) and amorphous (11%) parts." @default.
• W2017460829 created "2016-06-24" @default.
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• W2017460829 date "2002-03-01" @default.
• W2017460829 modified "2023-09-25" @default.
• W2017460829 title "Characterization of Mechanically Attrited Si/SiO<i>_x</i> Nanoparticles and Their Self-Assembled Composite Films" @default.
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• W2017460829 doi "https://doi.org/10.1021/cm010362l" @default.
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