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- W2017481916 abstract "A novel method for the synthesis of (2-pyridyl)alanines 2a−b was developed by converting (2-pyridyl)dehydroamino acid derivatives 1a−b to the corresponding N-oxides 3a−b followed by asymmetric hydrogenation using (R,R)-[Rh(Et-DUPHOS)(COD)]BF4 [(R,R)-6] catalyst and subsequent N-oxide reduction in 80−83% ee. This methodology was applied to the total synthesis of l-azatyrosine [(+)-12], an antitumor antibiotic, starting from (5-benzyloxy)-2-pyridylmethanol (7), in >96% enantiomeric purity." @default.
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- W2017481916 date "2001-09-07" @default.
- W2017481916 modified "2023-10-03" @default.
- W2017481916 title "Enantioselective Synthesis of (2-Pyridyl)alanines via Catalytic Hydrogenation and Application to the Synthesis of <scp>l</scp>-Azatyrosine" @default.
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- W2017481916 doi "https://doi.org/10.1021/ol016455q" @default.
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