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- W2017603121 abstract "In situ small-angle X-ray diffraction (SAXD) investigations are carried out in order to obtain an insight into the formation process of 2D hexagonal ordered phenylene- and thiophene-bridged periodic mesoporous organosilicas (PMOs) synthesized with Brij 76 (polyethylene (10) stearylether). The reaction solution is investigated by pumping it through a capillary placed in a synchrotron radiation beam. Data collection is stopped when the growing particle size lead to an irregular flow of the solution. The resulting data is compared with powder X-ray diffraction of the samples synthesized in the laboratory. The 2D hexagonal ordered PMO products synthesized with Brij 76 are formed via a metastable three-dimensional hexagonal ordered transition state. Here, we describe the formation process of the PMO materials regarding the properties of the structure-directing agent." @default.
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- W2017603121 date "2010-05-24" @default.
- W2017603121 modified "2023-10-12" @default.
- W2017603121 title "In situ SAXD Studies on Phenylene- and Thiophene-Bridged Periodic Mesoporous Organosilicas (PMOs)" @default.
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- W2017603121 doi "https://doi.org/10.1021/cm100673s" @default.
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