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- W2017614753 abstract "Several mucolipid preparations from ox brain were studied with respect to their long-chain base and fatty acid constituents. The mixture of bases, released by acid methanolysis and isolated in the form of the neutral oxalates, was subjected to oxidative degradation by means of HIO4, OsO4-HIO4, KMnO4, and CrO3. The analysis by gasliquid chromatography of the reaction products or their derivatives demonstrated the occurrence of two principal long-chain constituents in almost equal quantities, namely, sphingosine and its C20 homologue, 2-amino-1,3-dihydroxy-n-eicosene-4, for which the name icosisphingosine is proposed, together with much smaller quantities of dihydrosphingosine, probably, dihydroicosisphingosine. Stearic acid was the principal fatty acid constituent of the mucolipids, amounting in the purest preparations to 96–97% of the total fatty acids. Orienting experiments on the fractionation of mucolipid, in the form of its methyl ester, on a silicic acid column led to the isolation of two fractions some of whose properties are also discussed. The two long-chain base constituents were found in both fractions." @default.
- W2017614753 created "2016-06-24" @default.
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- W2017614753 date "1965-02-01" @default.
- W2017614753 modified "2023-09-25" @default.
- W2017614753 title "Studies on the chemistry of mucolipids: Occurrence of the long-chain base icosisphingosine, composition of fatty acids, fractionation attempts" @default.
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- W2017614753 doi "https://doi.org/10.1016/0005-2760(65)90021-4" @default.
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