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- W2017657301 endingPage "126" @default.
- W2017657301 startingPage "118" @default.
- W2017657301 abstract "The pseudocalixarene tetraiminotetraphenol macrocyclic ligand H4L has been structurally characterized and used to synthesize the complexes [FeIII2L(NO3)2(H2O)2] (1), [FeIII2L(Cl)2]∞ (2), [{FeIII2L(μ-O)}2]·2CH3CN·H2O (3), [MnIII2L(Cl)2]·3H2O (4) and [MnIII2L(OAc)2]·5H2O (5). The crystal structures of 3 and 4 have been determined. Variable-temperature (2–295 K) magnetic susceptibility measurements have been carried out for 3 and the data have been fitted to the spin Hamiltonian H = −2JS1.S2 with J = −45 cm−1. Cyclic voltammetric measurements carried out for 1 in N,N-dimethylformamide have revealed the presence of two reversible redox couples with E1/2 = −180 and −280 mV, which coalesced into a single couple with E1/2 = −220 mV with the addition of excess NaNO3. The two manganese(III) complexes undergo quasi-reversible reduction in methanol at the same potential with E1/2 = −240 mV." @default.
- W2017657301 created "2016-06-24" @default.
- W2017657301 creator A5013307190 @default.
- W2017657301 creator A5038983115 @default.
- W2017657301 creator A5076026985 @default.
- W2017657301 creator A5076909165 @default.
- W2017657301 creator A5087967838 @default.
- W2017657301 date "2014-06-01" @default.
- W2017657301 modified "2023-10-01" @default.
- W2017657301 title "Iron(III) and manganese(III) complexes of a pseudocalixarene tetraiminotetraphenol macrocyclic ligand: Structure, magnetism and electrochemistry" @default.
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