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• W2017695905 abstract "The structures of fi ve clinopyroxenes on the diopside–enstatite join have been refi ned by Rietveld analysis of powder-diffraction patterns obtained with synchrotron radiation. The reliability of the present Rietveld refi nements was checked against previous single-crystal data on the sample with composition Di80En20, and it showed reasonable agreement. A difference in the y/b M2 coordinate is related to the lower resolution of the powder-diffraction data of this work, not suffi cient to detect the splitting at the M2 site. The Rietveld analysis allowed us to detect the strain modulations on (010) prior to exsolution. The small size of primitive antiphase domains, less than the length-scale of X-ray diffraction, prevents P21/c refi nement in samples with composition Di59En41 and Di52En42CaTs2. The refi ned clinopyroxenes encompass the transition from P21/c to C2/c structures. In the P21/c structure, the A and B chains of tetrahedra undergo a slight straightening with increasing Ca content, and changes similar to those observed at high temperature. The results are in general agreement with large changes in the confi guration of the chains at the transition, as observed during the P21/c – C2/c transition at high pressure and high temperature." @default.
• W2017695905 created "2016-06-24" @default.
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• W2017695905 date "2005-08-01" @default.
• W2017695905 modified "2023-10-07" @default.
• W2017695905 title "RIETVELD REFINEMENT OF CLINOPYROXENES WITH INTERMEDIATE Ca-CONTENT ALONG THE JOIN DIOPSIDE ENSTATITE" @default.
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• W2017695905 doi "https://doi.org/10.2113/gscanmin.43.4.1411" @default.
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