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• W2017709012 abstract "The carbonyl derivatized bis(alkyne) OC(4-C6H4OCH2CCH)2 was converted into the imine derivatives RNC(4-C6H4OCH2CCH)2 [R=OH, NHC(O)NH2, NHC6H3-2,4-(NO2)2] and into the 4-bromomethyl-1,3-dioxolane derivative BrCH2C2H3O2C(4-C6H4OCH2CCH)2. The alkyne units in these compounds react with [AuCl(SMe2)] in the presence of base to form the corresponding digold(I) diacetylide complexes, that exist as insoluble oligomers or polymers. They reacted with the diphosphines Ph2PZPPh2 [Z=CC, trans-HCCH and (CH2)n, n=3–5] to give macrocyclic gold(I) complexes of the type [Au2(μ-LL)(μ-PP)], where LL is the diacetylide and PP the diphosphine ligand. The ability of these macrocyclic complexes to self-assemble to [2]catenanes has been studied. The ketone and imine derivatives do not form [2]catenanes because the orientation of the aryl groups is unfavorable, but the 1,3-dioxolane derivatives may catenate if the ring size is optimum." @default.
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• W2017709012 date "2003-03-01" @default.
• W2017709012 modified "2023-10-10" @default.
• W2017709012 title "Macrocyclic gold(I) complexes and [2]catenanes containing carbonyl functionalized diacetylide ligands" @default.
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• W2017709012 doi "https://doi.org/10.1016/s0022-328x(02)02070-3" @default.
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