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• W2017804303 abstract "Abstract The potentiostatic electroreduction of anodic layers containing Pb(II)-species formed on lead has been investigated in 5 M H 2 SO 4 at 25°C. By properly adjusting both the anodic layer formation and the electroreduction conditions three well-defined processes could be distinguished. (i) The electroreduction of the primary PbSO 4 layer which involves mainly an instantaneous nucleation and three-dimensional growth mechanism under diffusion control. (ii) The electroreduction of the PbO layer, which builds up progressively beneath the initially grown PbSO 4 porous layer, consists of two current contributions; one term can be associated with an instantaneous nucleation and 2D growth under diffusion control and the other one, which is the main current contribution, can be related to a progressive nucleation and 3D growth mechanism under charge transfer control. The latter includes a death correction term for either the growing or the disappearing right circular cones phase centres. (iii) The electroreduction of the composite PbSO 4 -PbO layer which can be successfully described in accordance with a complex mechanism by taking into account the simultaneous influence of the two single surface layer constituents." @default.
• W2017804303 created "2016-06-24" @default.
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• W2017804303 date "1992-05-01" @default.
• W2017804303 modified "2023-09-26" @default.
• W2017804303 title "Kinetics and mechanism of the electroreduction of anodic layers formed on lead in 5 M H2SO4 at 25°C" @default.
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• W2017804303 doi "https://doi.org/10.1016/0013-4686(92)85232-a" @default.
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